Pct after test and eq cycle

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From 1991-2005 I worked at this charity in IT, first as a programmer analyst, then as a dba, finally becoming the backup Unix Admin in 1998 and the full time Unix Admin in 2000. The organization ran its legacy fund raising systems on a pair of D class HP-UX systems. The back end database was Software AG adabas. The user fund raising community wanted to have an sql like ability to look into the database and run queries. they wanted flexible use of strategic data. An attempt was made in early 1997 to install a sql front end, but it did not provide acceptable results.

A suspension of mmole ( g) of 1,3-bis(2-chloroethyl)urea in 8 ml methylene dichloride at -10° C. was saturated with dinitrogen trioxide in 20% excess of theoretical. The heterogeneous mixture gradually changed to a green homogeneous solution. The methylene dichloride was evaporated, and the residue was extracted with 3× 10 ml hexane. Evaporation of the hexane gave g of oil which was the crude BCNU (NSC 409962). The hexane insoluble portion, g, when treated with benzene, gave g of 1,3-bis(2-chloroethyl)urea which was benzene insoluble. The benzene solubles were processed through a silica column (1× 10 cm) and g of crude BCNU was obtained. The combined fractions of crude product amounted to g (%).

Pct after test and eq cycle

pct after test and eq cycle


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